HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chlorophenyl)-2-methyl-3-furaldehyde → 1-[5-(4-Chlorophenyl)-2-methyl-3-furyl]-3-methylbutan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chlorophenyl)-2-methyl-3-furaldehyde | HCID 21986471 | — |
| Solvent | HCID 178420648 | HCID 178420648 | — |
| Product | 1-[5-(4-Chlorophenyl)-2-methyl-3-furyl]-3-methylbutan-1-ol | HCID 68512627 | 170.5% |
Reaction Steps
An operation similar to that in Example 3 (2) was performed using 5-(4-chlorophenyl)-2-methyl-3-furaldehyde (1.3 g) and 1N isobutylmagnesium bromide-tetrahydrofuran solution (10 mL) to give the title compound (1.4 g, 85%) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-a8557d7ed0d441caaabc4bed5d807053 |
| Source note | uspto-grants-2012_11 |