HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chlorophenyl)-2-methyl-3-furaldehyde → [5-(4-Chlorophenyl)-2-methyl-3-furyl](cyclohexyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chlorophenyl)-2-methyl-3-furaldehyde | HCID 21986471 | — |
| Reactant | HCID 178420632 | HCID 178420632 | — |
| Product | [5-(4-Chlorophenyl)-2-methyl-3-furyl](cyclohexyl)methanol | HCID 68509840 | 83% |
Reaction Steps
An operation similar to that in Example 3 (2) was performed using 5-(4-chlorophenyl)-2-methyl-3-furaldehyde (1.7 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (15 mL) to give the title compound (2.0 g, 83%) as a white crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-922c2f337ed144208328425921ca39fd |
| Source note | uspto-grants-2012_11 |