HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl acetoacetate → HCID 22261473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl acetoacetate | HCID 7757 | — |
| Reactant | 2-Chloro-4'-fluoroacetophenone | HCID 120248 | — |
| Product | HCID 22261473 | HCID 22261473 | 63% |
Reaction Steps
An operation similar to that in Example 1 (1) was performed using 2-chloro-4′-fluoroacetophenone (13.4 g) and methyl acetoacetate (8.6 g) to give the title compound (7.4 g, 63%) as a yellow crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-9a790d56ccf44914a3c6d2b0fd85c9dc |
| Source note | uspto-grants-2012_11 |