HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(2,4-Dichlorophenyl)-2-methyl-3-furaldehyde → Cyclohexyl[5-(2,4-dichlorophenyl)-2-methyl-3-furyl]methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(2,4-Dichlorophenyl)-2-methyl-3-furaldehyde | HCID 83595757 | — |
| Reactant | HCID 178420632 | HCID 178420632 | — |
| Product | Cyclohexyl[5-(2,4-dichlorophenyl)-2-methyl-3-furyl]methanol | HCID 68511587 | 77% |
Reaction Steps
An operation similar to that in Example 3 (2) was performed using 5-(2,4-dichlorophenyl)-2-methyl-3-furaldehyde (1.3 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (7.5 mL) to give the title compound (1.3 g, 77%) as a white crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-85cadfcc69ef4610a00e4d6ba7420bfb |
| Source note | uspto-grants-2012_11 |