HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Fluoro-2-methylphenyl)-2-methyl-3-furaldehyde → Cyclohexyl[5-(4-fluoro-2-methylphenyl)-2-methyl-3-furyl]methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Fluoro-2-methylphenyl)-2-methyl-3-furaldehyde | HCID 86646367 | — |
| Reactant | HCID 178420632 | HCID 178420632 | — |
| Product | Cyclohexyl[5-(4-fluoro-2-methylphenyl)-2-methyl-3-furyl]methanol | HCID 68515490 | 72% |
Reaction Steps
An operation similar to that in Example 3 (2) was performed using 5-(4-fluoro-2-methylphenyl)-2-methyl-3-furaldehyde (2.6 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (18 mL) to give the title compound (2.6 g, 72%) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-16a088323c3a4b889b0e46625ec3144b |
| Source note | uspto-grants-2012_11 |