HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Tert-butyl-2-methylfuran-3-carbaldehyde → (5-Tert-butyl-2-methyl-3-furyl)(cyclohexyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Tert-butyl-2-methylfuran-3-carbaldehyde | HCID 57437981 | — |
| Reactant | HCID 178420632 | HCID 178420632 | — |
| Product | (5-Tert-butyl-2-methyl-3-furyl)(cyclohexyl)methanol | HCID 68514163 | 62% |
Reaction Steps
An operation similar to that in Example 3 (2) was performed using 5-tert-butyl-2-methyl-3-furaldehyde (2.5 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (23 mL) to give the title compound (2.3 g, 62%) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-4dfba799bc9545f4b4c44ed9c763f791 |
| Source note | uspto-grants-2012_11 |