Thionyl Chloride → HCID 68515497, compound

HRID 1877062Notes

Reaction equation

HRID 1877062 reaction equation
[CH3:1][CH:2]([CH3:18])[CH2:3][CH:4]([C:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[O:8][C:7]=1[CH3:17])O.S(Cl)([Cl:21])=O>C1(C)C=CC=CC=1>[Cl:21][CH:4]([C:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[O:8][C:7]=1[CH3:17])[CH2:3][CH:2]([CH3:18])[CH3:1]

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 685095783-Methyl-1-(2-methyl-5-phenylfuran-3-yl)butan-1-ol

Product 1

HCID 68515497HCID 68515497, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

To a solution of 3-methyl-1-(2-methyl-5-phenylfuran-3-yl)butan-1-ol (1.5 g) in toluene (20 mL) was added thionyl chloride (0.9 mL), and the mixture was stirred at room temperature overnight. The solvent was evaporated under reduced pressure to give the title compound (1.6 g, 100%) as an oil.

Workup

  1. customThe solvent was evaporated under reduced pressure

Sources & evidence

ORD record
ord-059cce386ae5449980b3c2710eff9d05
Source dataset
uspto-grants-2012_11
Patent number
US08309580B2

Reaction notes

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