Thionyl Chloride → HCID 68515145, compound

HRID 1877068Notes

Reaction equation

HRID 1877068 reaction equation
[CH3:1][C:2]1[O:3][C:4]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:5][C:6]=1[CH:7](O)[CH2:8][CH2:9][CH2:10][CH3:11].S(Cl)([Cl:21])=O>C1(C)C=CC=CC=1>[Cl:21][CH:7]([C:6]1[CH:5]=[C:4]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[O:3][C:2]=1[CH3:1])[CH2:8][CH2:9][CH2:10][CH3:11]

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 68511412HCID 68511412, compound

Product 1

HCID 68515145HCID 68515145, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

To a solution of 1-(2-methyl-5-phenylfuran-3-yl)pentan-1-ol (1.6 g) in toluene (20 mL) was added thionyl chloride (1.0 mL), and the mixture was stirred at room temperature overnight. The solvent was evaporated under reduced pressure to give the title compound (1.7 g, 100%) as an oil.

Workup

  1. customThe solvent was evaporated under reduced pressure

Sources & evidence

ORD record
ord-65cfa14fcbe84f95af5ba79ad8d7189f
Source dataset
uspto-grants-2012_11
Patent number
US08309580B2

Reaction notes

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