Thionyl Chloride → HCID 68509127, compound

HRID 1877071Notes

Reaction equation

HRID 1877071 reaction equation
[CH3:1][C:2]([CH3:19])([CH3:18])[CH2:3][CH:4]([C:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[O:8][C:7]=1[CH3:17])O.S(Cl)([Cl:22])=O>C1(C)C=CC=CC=1>[Cl:22][CH:4]([C:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[O:8][C:7]=1[CH3:17])[CH2:3][C:2]([CH3:19])([CH3:18])[CH3:1]

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 685133603,3-Dimethyl-1-(2-methyl-5-phenylfuran-3-yl)butan-1-ol

Product 1

HCID 68509127HCID 68509127, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

To a solution of 3,3-dimethyl-1-(2-methyl-5-phenylfuran-3-yl)butan-1-ol (1.1 g) in toluene (15 mL) was added thionyl chloride (0.6 mL), and the mixture was stirred at room temperature overnight. The solvent was evaporated under reduced pressure to give the title compound (1.1 g, 100%) as an oil.

Workup

  1. customThe solvent was evaporated under reduced pressure

Sources & evidence

ORD record
ord-1324460f941843fd8d3253a37b00e7a8
Source dataset
uspto-grants-2012_11
Patent number
US08309580B2

Reaction notes

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