HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chlorophenylhydrazine hydrochloride → HCID 58345403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chlorophenylhydrazine hydrochloride | HCID 75331 | — |
| Reactant | HCID 58277306 | HCID 58277306 | — |
| Product | HCID 58345403 | HCID 58345403 | 35% |
Reaction Steps
Starting from 10 g (39.81 mmol) of lithium (1Z)-1-(3-cyanophenyl)-4-ethoxy-3,4-dioxobut-1-en-1-olate from example 10A and 9.7 g (54.15 mmol) of 3-chlorophenylhydrazine hydrochloride, 4.97 g (14 mmol, 35% yield of theory) of product are obtained according to the method described in example 4A.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314089B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-d5cec886890c412388fec8fc3787926d |
| Source note | uspto-grants-2012_11 |