HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,5-Dimethylphenyl)piperazine → HCID 52947129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,5-Dimethylphenyl)piperazine | HCID 2758626 | — |
| Reactant | Ethyl N-(6-chloro-2-methoxyquinoxalin-3-yl)carbamate | HCID 66918182 | — |
| Product | HCID 52947129 | HCID 52947129 | 79% |
Reaction Steps
Ethyl N-(6-chloro-2-methoxyquinoxalin-3-yl)carbamate and 1-(3,5-dimethylphenyl)piperazine were reacted by the same way with the example 22 to obtain the titled compound (yield, 79%). 1H NMR (300 MHz, CDCl3): δ 2.29 (s, 6H), 3.19-3.29 (m, 4H), 3.73-3.89 (m, 3H), 4.11-4.14 (m, 4H), 6.58 (s, 3H), 7.19-7.25 (m, 1H), 7.36-7.64 (m, 2H), 7.67-7.81 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314100B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-0691a58c6349470cb4374abac0c3aed5 |
| Source note | uspto-grants-2012_11 |