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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878134Generated: November 2, 2026

1-(4-Chlorophenyl)piperazine → HCID 66918076, compound

https://huagongshe.com/reaction/1878134

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(4-Chlorophenyl)piperazineHCID 97478—
ReactantEthyl N-(6-chloro-2-methoxyquinoxalin-3-yl)carbamateHCID 66918182—
ProductHCID 66918076HCID 6691807696%

Reaction Steps

Ethyl N-(6-chloro-2-methoxyquinoxalin-3-yl)carbamate and 1-(4-chlorophenyl)piperazine were reacted by the same way with the example 22 to obtain the titled compound (yield, 96%). 1H NMR (300 MHz, CDCl3): δ 3.18-3.26 (m, 4H), 3.76 (s, 3H), 4.11-4.14 (m, 4H), 6.84-6.87 (d, J=8.7 Hz, 2H), 7.22-7.34 (m, 3H), 7.41-7.53 (m, 1H), 7.65-7.66 (m, 1H), 7.79 (s, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314100B2
Source datasetuspto-grants-2012_11
ORD IDord-9463919614f34fb4b9dac0f04c7e13eb
Source noteuspto-grants-2012_11