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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878138Generated: November 1, 2026

1-(2-Pyridyl)piperazine → HCID 66918237, compound

https://huagongshe.com/reaction/1878138

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(2-Pyridyl)piperazineHCID 94459—
ReactantEthyl N-(6-chloro-2-methoxyquinoxalin-3-yl)carbamateHCID 66918182—
ProductHCID 66918237HCID 6691823770%

Reaction Steps

Ethyl N-(6-chloro-2-methoxyquinoxalin-3-yl)carbamate and 1-(2-pyridyl)piperazine were reacted by the same way with the example 22 to obtain the titled compound (yield, 70%), 1H NMR (300 MHz, CDCl3): δ 3.63-3.73 (m, 7H), 4.08-4.15 (m, 4H), 6.68 (d, J=8.7 Hz, 2H), 7.20-7.31 (m, 1H), 7.42-7.53 (m, 2H), 7.65-7.80 (m, 2H), 8.21 (d, J=3.6 Hz, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314100B2
Source datasetuspto-grants-2012_11
ORD IDord-46fc609409284fadbb0f7401c8de03fa
Source noteuspto-grants-2012_11