HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,4,5-Trimethoxyphenyl)piperazine → HCID 66917985, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,4,5-Trimethoxyphenyl)piperazine | HCID 3838765 | — |
| Reactant | Ethyl N-(2-methoxy-6-methylquinoxalin-3-yl)carbamate | HCID 66917958 | — |
| Product | HCID 66917985 | HCID 66917985 | 94% |
Reaction Steps
Ethyl N-(2-methoxy-6-methylquinoxalin-3-yl)carbamate and 1-(3,4,5-trimethoxyphenyl)piperazine were reacted by the same way with the example 43 to obtain the titled compound (yield, 94%). 1H NMR (300 MHz, CDCl3): δ 2.44-2.49 (m, 3H), 3.18-3.25 (m, 4H), 3.80-3.86 (m, 12H), 4.04-4.13 (m, 4H), 6.20 (s, 2H), 7.02-7.20 (m, 1H), 7.31-7.40 (m, 1H), 7.46-7.63 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314100B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-021a6220b5644cffaecb8f2e2860146c |
| Source note | uspto-grants-2012_11 |