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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878150Generated: November 1, 2026

1-(2,6-Xylyl)piperazine → HCID 66918125, compound

https://huagongshe.com/reaction/1878150

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(2,6-Xylyl)piperazineHCID 70538—
ReactantEthyl N-(2-methoxy-6-methylquinoxalin-3-yl)carbamateHCID 66917958—
ProductHCID 66918125HCID 6691812588%

Reaction Steps

Ethyl N-(2-methoxy-6-methylquinoxalin-3-yl)carbamate and 1-(2,6-dimethylphenyl)piperazine were reacted by the same way with the example 43 to obtain the titled compound (yield, 88%). 1H NMR (300 MHz, CDCl3): δ 2.04-2.58 (m, 9H), 3.14-3.20 (m, 4H), 3.71-3.76 (m, 3H), 4.07-4.14 (m, 4H), 7.00-7.15 (m, 4H), 7.25-7.76 (m, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314100B2
Source datasetuspto-grants-2012_11
ORD IDord-1eba1e6ed7b3483ca949ca4710351100
Source noteuspto-grants-2012_11