HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Fluorophenyl)piperazine → HCID 66917992, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Fluorophenyl)piperazine | HCID 75260 | — |
| Reactant | Ethyl N-(2-methoxy-6-methylquinoxalin-3-yl)carbamate | HCID 66917958 | — |
| Product | HCID 66917992 | HCID 66917992 | 70% |
Reaction Steps
Ethyl N-(2-methoxy-6-methylquinoxalin-3-yl)carbamate and 1-(4-fluorophenyl)piperazine were reacted by the same way with the example 43 to obtain the titled compound (yield, 70%). 1H NMR (300 MHz, CDCl3): δ 2.43-2.49 (m, 3H), 3.13-3.21 (m, 4H), 3.77 (s, 3H), 4.11-4.13 (m, 4H), 6.88-6.99 (m, 4H), 7.13 (m, 1H), 7.25 (m, 1H), 7.48-7.65 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314100B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-1c22279956884a52ac1e30a37f284c02 |
| Source note | uspto-grants-2012_11 |