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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878160Generated: November 2, 2026

1-(2-Pyridyl)piperazine → HCID 66917964, compound

https://huagongshe.com/reaction/1878160

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(2-Pyridyl)piperazineHCID 94459—
ReactantEthyl N-(2-methoxy-6-methylquinoxalin-3-yl)carbamateHCID 66917958—
ProductHCID 66917964HCID 6691796483%

Reaction Steps

Ethyl N-(2-methoxy-6-methylquinoxalin-3-yl)carbamate and 1-(2-pyridyl)piperazine were reacted by the same way with the example 43 to obtain the titled compound (yield, 83%). 1H NMR (300 MHz, CDCl3): δ 2.43-2.47 (m, 3H), 3.63-3.73 (m, 7H), 4.13 (s, 4H), 6.67 (d, J=8.4 Hz, 2H), 7.01-7.12 (m, 1H), 7.30-7.33 (m, 1H), 7.48-7.62 (m, 3H), 8.21 (dd, J=4.8 and 1.5 Hz, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314100B2
Source datasetuspto-grants-2012_11
ORD IDord-368cb14a169f47f18cbb8d60ba84b420
Source noteuspto-grants-2012_11