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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1878170Erstellt: 25. Oktober 2026

1-(m-Tolyl)piperazine → 1-[(2,6-Dimethoxyquinoxalin-3-yl)aminocarbonyl]-4-(3-methylphenyl)piperazine

https://huagongshe.com/reaction/1878170

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-(m-Tolyl)piperazineHCID 83111—
EduktEthyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamateHCID 66918080—
Produkt1-[(2,6-Dimethoxyquinoxalin-3-yl)aminocarbonyl]-4-(3-methylphenyl)piperazineHCID 6691798995%

Reaktionsschritte

Ethyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamate and 1-(3-methylphenyl)piperazine were reacted by the same way with the example 64 to obtain the titled compound (yield, 95%). 1H NMR (300 MHz, CDCl3): δ 2.33 (s, 3H), 3.26 (s, 4H), 3.72-3.89 (m, 6H), 4.09-4.18 (m, 4H), 6.72-6.78 (m, 4H), 7.03-7.37 (m, 3H), 7.57-7.65 (m, 1H).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08314100B2
Quelldatensatzuspto-grants-2012_11
ORD IDord-90c0d2d519ca4923becc219680d03136
Quellennotizuspto-grants-2012_11