HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(m-Tolyl)piperazine → 1-[(2,6-Dimethoxyquinoxalin-3-yl)aminocarbonyl]-4-(3-methylphenyl)piperazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(m-Tolyl)piperazine | HCID 83111 | — |
| Edukt | Ethyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamate | HCID 66918080 | — |
| Produkt | 1-[(2,6-Dimethoxyquinoxalin-3-yl)aminocarbonyl]-4-(3-methylphenyl)piperazine | HCID 66917989 | 95% |
Reaktionsschritte
Ethyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamate and 1-(3-methylphenyl)piperazine were reacted by the same way with the example 64 to obtain the titled compound (yield, 95%). 1H NMR (300 MHz, CDCl3): δ 2.33 (s, 3H), 3.26 (s, 4H), 3.72-3.89 (m, 6H), 4.09-4.18 (m, 4H), 6.72-6.78 (m, 4H), 7.03-7.37 (m, 3H), 7.57-7.65 (m, 1H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08314100B2 |
| Quelldatensatz | uspto-grants-2012_11 |
| ORD ID | ord-90c0d2d519ca4923becc219680d03136 |
| Quellennotiz | uspto-grants-2012_11 |