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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878171Generated: November 2, 2026

1-(2,6-Xylyl)piperazine → HCID 66918084, compound

https://huagongshe.com/reaction/1878171

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(2,6-Xylyl)piperazineHCID 70538—
ReactantEthyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamateHCID 66918080—
ProductHCID 66918084HCID 6691808487%

Reaction Steps

Ethyl N-(2,6-dimethoxyquinoxalin-3-yl)carbamate and 1-(2,6-dimethylphenyl)piperazine were reacted by the same way with the example 64 to obtain the titled compound (yield, 87%). 1H NMR (300 MHz, CDCl3): δ 2.33-2.36 (m, 6H), 3.14-3.22 (m, 4H), 3.70-3.90 (m, 6H), 4.09-4.15 (m, 4H), 6.67-7.32 (m, 6H), 7.50-7.65 (m, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314100B2
Source datasetuspto-grants-2012_11
ORD IDord-1f070d8922f84e858451f759e9fbae48
Source noteuspto-grants-2012_11