HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-methoxyphenyl)piperazine → HCID 69243624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-methoxyphenyl)piperazine | HCID 81430 | — |
| Reactant | ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate | HCID 69241674 | — |
| Product | HCID 69243624 | HCID 69243624 | 85% |
Reaction Steps
Ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate and 1-(3-methoxyphenyl)piperazine were reacted by the same way with the example 106 to obtain the titled compound (yield, 85%). 1H NMR (300 MHz, CDCl3): δ 3.14-3.16 (m, 4H), 3.76-3.80 (m, 7H), 4.14 (s, 3H), 6.46-6.58 (m, 3H), 7.14-7.44 (m, 3H), 7.62-7.74 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314100B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-52b7b8c0a0184dc2ab2a20ce9ea2482d |
| Source note | uspto-grants-2012_11 |