HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,4,5-Trimethoxyphenyl)piperazine → HCID 69243801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,4,5-Trimethoxyphenyl)piperazine | HCID 3838765 | — |
| Reactant | ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate | HCID 69241674 | — |
| Product | HCID 69243801 | HCID 69243801 | 83% |
Reaction Steps
Ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate and 1-(3,4,5-trimethoxyphenyl)piperazine were reacted by the same way with the example 106 to obtain the titled compound (yield, 83%). 1H NMR (300 MHz, CDCl3): 3.24 (s, 4H), 3.81-3.86 (m, 12H), 4.15 (s, 3H), 6.21 (s, 2H), 7.36-7.45 (m, 1H), 7.27 (s, 1H), 7.36-7.45 (m, 1H), 7.64-7.75 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314100B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-b4433bd0784044e89ff963cddfc63fc2 |
| Source note | uspto-grants-2012_11 |