HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Chlorophenyl)piperazine → HCID 69244533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Chlorophenyl)piperazine | HCID 415628 | — |
| Reactant | ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate | HCID 69241674 | — |
| Product | HCID 69244533 | HCID 69244533 | 91% |
Reaction Steps
Ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate and 1-(2-chlorophenyl)piperazine were reacted by the same way with the example 106 to obtain the titled compound (yield, 91%). 1H NMR (300 MHz, CDCl3): δ 3.15 (s, 4H), 3.79 (s, 4H), 4.15 (s, 3H), 6.99-7.06 (m, 2H), 7.23-7.45 (m, 4H), 7.74-7.79 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314100B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-c1809d823af44a9d965d8cf58ede3194 |
| Source note | uspto-grants-2012_11 |