HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2,6-Xylyl)piperazine → HCID 69245227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2,6-Xylyl)piperazine | HCID 70538 | — |
| Reactant | ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate | HCID 69243736 | — |
| Product | HCID 69245227 | HCID 69245227 | 83% |
Reaction Steps
Ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate and 1-(2,6-dimethylphenyl)piperazine were reacted by the same way with the example 127 to obtain the titled compound (yield, 83%). 1H NMR (300 MHz, CDCl3): δ 2.33-2.50 (m, 9H), 3.14-2.20 (m, 4H), 3.70-3.75 (m, 4H), 4.14 (s, 3H), 7.00 (s, 3H), 7.09-7.78 (m, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314100B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-8f38189258464e1697a37b37ac8ba18e |
| Source note | uspto-grants-2012_11 |