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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878246Generated: November 1, 2026

1-(4-Chlorophenyl)piperazine → HCID 69242307, compound

https://huagongshe.com/reaction/1878246

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(4-Chlorophenyl)piperazineHCID 97478—
Reactantethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamateHCID 69243736—
ProductHCID 69242307HCID 6924230791%

Reaction Steps

Ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate and 1-(4-chlorophenyl)piperazine were reacted by the same way with the example 127 to obtain the titled compound (yield, 91%). 1H NMR (300 MHz, CDCl3): δ 2.50 (s, 3H), 3.18-3.28 (m, 4H), 3.73-3.78 (m, 4H), 4.14 (s, 3H), 6.86 (dd, J=12.2 Hz, 2H), 7.00-7.60 (m, 5H), 7.71 (d, J=8.2 Hz, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314100B2
Source datasetuspto-grants-2012_11
ORD IDord-25e50e230c0d4db99d6b8e4241b7d2f0
Source noteuspto-grants-2012_11