HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazin-4-ylacetophenone → HCID 69243973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazin-4-ylacetophenone | HCID 97269 | — |
| Reactant | ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate | HCID 69243736 | — |
| Product | HCID 69243973 | HCID 69243973 | 97% |
Reaction Steps
Ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate and 1-(4-acetylphenyl)piperazine were reacted by the same way with the example 127 to obtain the titled compound (yield, 97%). 1H NMR (300 MHz, CDCl3): δ 2.17 (s, 3H), 2.54 (s, 3H), 3.39-3.58 (m, 4H), 3.71-3.90 (m, 4H), 4.14 (s, 3H), 6.89 (d, J=6.4 Hz, 2H), 7.21-7.54 (m, 4H), 7.90 (d, J=6.4 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314100B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-7b34d9e73018494ba9ced2111fb0cd8c |
| Source note | uspto-grants-2012_11 |