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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1878262Generated: October 31, 2026

1-(2,6-Xylyl)piperazine → HCID 69240983, compound

https://huagongshe.com/reaction/1878262

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(2,6-Xylyl)piperazineHCID 70538—
Reactantethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamateHCID 69244324—
ProductHCID 69240983HCID 6924098391%

Reaction Steps

Ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate and 1-(2,6-dimethylphenyl)piperazine were reacted by the same way with the example 148 to obtain the titled compound (yield, 91%). 1H NMR (300 MHz, CDCl3): δ 2.36 (s, 6H), 3.17-3.21 (m, 4H), 3.68-3.71 (m, 4H), 3.91 (s, 3H), 4.14 (s, 3H), 6.95-7.03 (m, 3H), 7.14-7.21 (m, 3H), 7.77-7.80 (m, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08314100B2
Source datasetuspto-grants-2012_11
ORD IDord-5acfd2c3377b474c93b8501225c36579
Source noteuspto-grants-2012_11