HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(m-Tolyl)piperazine → 1-[(2,6,7-Trimethoxyquinoxalin-3-yl)aminocarbonyl]-4-(3-methylphenyl)piperazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(m-Tolyl)piperazine | HCID 83111 | — |
| Edukt | HCID 69244380 | HCID 69244380 | — |
| Produkt | 1-[(2,6,7-Trimethoxyquinoxalin-3-yl)aminocarbonyl]-4-(3-methylphenyl)piperazine | HCID 69244359 | 56% |
Reaktionsschritte
Ethyl N-(2,6,7-trimethoxyquinoxalin-3-yl)carbamate and 1-(3-methylphenyl)piperazine were reacted by the same way with the example 190 to obtain the titled compound (yield, 56%). 1H NMR (300 MHz, CDCl3) δ 2.34 (s, 3H), 3.25-3.30 (m, 4H), 3.76-3.80 (m, 4H), 3.98 (s, 3H), 4.02 (s, 3H), 4.16 (s, 3H), 6.74-6.78 (m, 3H), 7.14-7.26 (m, 4H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08314100B2 |
| Quelldatensatz | uspto-grants-2012_11 |
| ORD ID | ord-f0dcf396bebf470aae535c6509369c24 |
| Quellennotiz | uspto-grants-2012_11 |