Acetic Acid → HCID 75216513, compound

Participants

Reaction Steps

There was suspended, in ethanol (1.0 mL), (7-morpholin-4-yl-2-pyrimidin-5-yl-pyrazolo[1,5-a]pyrimidin-5-yl)-hydrazine (18 mg, 0.1 mM) prepared in the preceding step 2, then acetic acid (3.0 μL, 0.05 mM) and metatolualdehyde (14 μL, 0.12 mM) were added to the suspension and the mixture was stirred at room temperature for 16 hours. The precipitated solid was recovered through filtration and then washed with diethyl ether to thus give the title compound (4.0 mg, yield: 16.7%).

Provenance & Evidence