HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isopropylbenzaldehyde → HCID 77933899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isopropylbenzaldehyde | HCID 520680 | — |
| Reactant | HCID 70867116 | HCID 70867116 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 77933899 | HCID 77933899 | 26.5% |
Reaction Steps
There was dissolved, in ethanol (2 mL), (7-morpholin-4-yl-2-pyridin-4-yl-pyrazolo[1,5-a]pyrimidin-5-yl)-hydrazine (30.1 mg, 0.0967 mM), then 3-isopropyl-benzaldehyde (14.3 mg, 0.0967 mM) was added to the solution and the mixture was stirred at room temperature overnight. The solvent was distilled off from this reaction liquid, the resulting residue was purified by the reversed phase HPLC and then subjected to a desalting treatment to thus give the title compound (11.3 mg, yield: 26%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314098B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-055a341b2fd14d15b0f9319f12ba2c77 |
| Source note | uspto-grants-2012_11 |