HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,6-Dichloropyridazine → HCID 24990110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,6-Dichloropyridazine | HCID 67331 | — |
| Reactant | HCID 14387348 | HCID 14387348 | — |
| Product | HCID 24990110 | HCID 24990110 | — |
Reaction Steps
Prepared from 1-azaadamantan-4-ol (3:2 diastereomer mixture; 150 mg, 0.979 mmol; see WO 9215579) and 3,6-dichloropyridazine (182 mg, 1.22 mmol; Aldrich) according to Method B to afford the title compound as a mixture of stereoisomers: MS (DCI/NH3) m/z=266 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314119B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-6854f079674a42faa244707ff58a183c |
| Source note | uspto-grants-2012_11 |