HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → HCID 57448044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-[2-Fluoro-3-(methylsulfonyl)phenyl]piperidine | HCID 57448038 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 57448044 | HCID 57448044 | — |
Reaction Steps
Preparation according to Example 1: 4-[2-fluoro-3-(methylsulfonyl)-phenyl]-piperidine (0.02 g, 0.078 mmol), acetonitrile (2 ml), potassium carbonate (0.02 g, 0.14 mmol), 1-bromobutane (0.009 ml, 0.082 mmol). MS m/z (relative intensity, 70 eV) 313 (M+, 2), 271 (14), 270 (bp), 147 (7) 133 (7).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314126B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-473ca4347187437783308c8a3e1c3566 |
| Source note | uspto-grants-2012_11 |