HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 11507445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 57448039 | HCID 57448039 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11507445 | HCID 11507445 | — |
Reaction Steps
Preparation according to Example 1: 4-[2-methyl-3-(methyl-sulfonyl)phenyl]piperidine (0.17 g, 0.67 mmol), acetonitrile (20 ml), potassium carbonate (0.23 g, 1.67 mmol) and 1-iodoethane (0.065 ml, 0.74 mmol). Yield: 0.12 g (64%). MS m/z (relative intensity, 70 eV) 281 (M+, 22), 267 (17), 266 (bp), 129 (12), 115 (24).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314126B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-8508bdd1e2134c1e9814a0e5a0208129 |
| Source note | uspto-grants-2012_11 |