HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 86085874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-{2-Fluoro-3-[(trifluoromethyl)sulfonyl]phenyl}piperidine | HCID 57448051 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86085874 | HCID 86085874 | — |
Reaction Steps
Preparation according to Example 18: 4-{2-fluoro-3-[(trifluoromethyl)sulfonyl]phenyl}-piperidine (0.01 g), acetonitrile (2 ml), potassium carbonate (0.01 g) and iodomethane (0.01 g). MS m/z (rel. intensity, 70 eV) 325 (M+, 63), 324 (bp), 305 (13), 191 (32), 133 (24).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314126B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-f508044062f64fdfaa25ccdab241747e |
| Source note | uspto-grants-2012_11 |