HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 57448062, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Sodium periodate | HCID 23667635 | — |
| Reactant | (3-Bromo-2-methylphenyl)(methyl)sulfane | HCID 57448061 | — |
| Catalyst | Ruthenium trichloride | HCID 61850 | — |
| Product | HCID 57448062 | HCID 57448062 | — |
Reaction Steps
Preparation according to preparation 4: 1-bromo-2-methyl-3-(methylthio)benzene (1.33 g), carbon tetrachloride (8 ml), acetonitrile (8 ml), water (16 ml), sodium periodate (3.9 g), ruthenium trichloride (1 mg). Yield: 1.6 g. MS m/z (rel. intensity, 70 eV) 250 (M+, 69), 248 (M+, 67), 169 (49), 90 (63), 89 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314126B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-d615e548032c4946ac30b0abc244da97 |
| Source note | uspto-grants-2012_11 |