HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 57448047, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 57448059 | HCID 57448059 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57448047 | HCID 57448047 | — |
Reaction Steps
Preparation according to preparation 6: 4-[2-chloro-3-(methylsulfonyl)phenyl]-pyridine (1.77 g, 6.6 mmol), 1-iodoethane (5 ml), ethanol (40 ml), sodium borohydride (2.2 g, 58 mmol). Yield: 0.6 g. MS m/z (rel. intensity, 70 eV) 300 (M+, 24), 299 (M+, 71), 298 (33), 284 (bp), 110 (74).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08314126B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-32a643fcb28d485da195a15f309c2ccf |
| Source note | uspto-grants-2012_11 |