HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-4-piperidone → 1-Methylpiperidin-4-one oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-4-piperidone | HCID 74049 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Product | 1-Methylpiperidin-4-one oxime | HCID 339053 | — |
Reaction Steps
1-Methyl-piperidin-4-one oxime was prepared from 1-methyl-piperidin-4-one and hydroxylamine hydrochloride using conditions of General Method 1. 1H NMR (400 MHz, DMSO-d6) δ 10.31 (1H, s), 2.45 (2H, t, 6.1 Hz), 2.38 (2H, t, 5.9 Hz), 2.31 (2H, t, J=6.0 Hz), 2.20 (2H, t, 6.4 Hz), 2.18 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318705B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-a7b52ff8ee0745ce932844be1e3b55b9 |
| Source note | uspto-grants-2012_11 |