HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → 1-(4-(Hydroxyimino)piperidin-1-yl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | N-Acetyl-4-piperidone | HCID 122563 | — |
| Product | 1-(4-(Hydroxyimino)piperidin-1-yl)ethanone | HCID 15707988 | — |
Reaction Steps
1-Acetyl-piperidin-4-one oxime was prepared from 1-acetyl-piperidin-4-one and hydroxylamine using conditions of General Method 1. 1H NMR (400 MHz, DMSO-d6) δ 10.48 (1H, d, 3.2 Hz), 3.43-3.56 (4H, m), 2.48-2.56 (1H, m), 2.42 (1H, t, 6.2 Hz), 2.29-2.34 (1H, m), 2.17-2.26 (1H, m), 2.03 (3H, d, 4.2 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318705B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-cf799b33388446cbb895efee779de907 |
| Source note | uspto-grants-2012_11 |