HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutyric Acid → 1-Methyl-4-nitrosopiperidin-4-yl isobutyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutyric Acid | HCID 6590 | — |
| Reactant | 1-Methylpiperidin-4-one oxime | HCID 339053 | — |
| Reactant | HCID 178418268 | HCID 178418268 | — |
| Product | 1-Methyl-4-nitrosopiperidin-4-yl isobutyrate | HCID 57954508 | — |
Reaction Steps
1-Methyl-4-nitrosopiperidin-4-yl isobutyrate was prepared from 1-methyl-piperidin-4-one oxime, lead tetraacetate and isobutyric acid using conditions of General Method 3. 1H NMR (400 MHz, chloroform-d) δ 2.82-2.94 (2H, m), 2.65 (1H, sept, 7.0 Hz), 2.36 (3H, s), 2.23-2.35 (4H, m), 1.83-1.92 (2H, m), 1.28 (3H, s), 1.27 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318705B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-ed7cd19135ac449db84755885950de72 |
| Source note | uspto-grants-2012_11 |