Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pivalic acid → 1-Methyl-4-nitrosopiperidin-4-yl pivalate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pivalic acid | HCID 6417 | — |
| 반응물 | 1-Methylpiperidin-4-one oxime | HCID 339053 | — |
| 반응물 | HCID 178418268 | HCID 178418268 | — |
| 생성물 | 1-Methyl-4-nitrosopiperidin-4-yl pivalate | HCID 57954464 | — |
반응 단계
1-Methyl-4-nitrosopiperidin-4-yl pivalate was prepared from 1-methyl piperidin-4-one oxime, lead tetraacetate and trimethylacetic acid using conditions of General Method 3. 1H NMR (400 MHz, CHLOROFORM-d) δ 2.86-3.00 (2H, m), 2.37 (3H, s), 2.21-2.35 (4H, m), 1.82-1.94 (2H, m), 1.32 (9H, s).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08318705B2 |
| 출처 데이터셋 | uspto-grants-2012_11 |
| ORD ID | ord-8e09ce58aef942aa91e359ba1fa6dc7e |
| 출처 메모 | uspto-grants-2012_11 |