Chromanone → HCID 59676133, compound

HRID 1880443Notes

Reaction equation

HRID 1880443 reaction equation
Cl.[CH2:2]([O:9][C:10]1[CH:15]=[CH:14][C:13]([NH:16]N)=[CH:12][CH:11]=1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[O:18]1[C:27]2[C:22](=[CH:23][CH:24]=[CH:25][CH:26]=2)[C:21](=O)[CH2:20][CH2:19]1>>[CH2:2]([O:9][C:10]1[CH:15]=[C:14]2[C:13](=[CH:12][CH:11]=1)[NH:16][C:21]1[C:22]3[CH:23]=[CH:24][CH:25]=[CH:26][C:27]=3[O:18][CH2:19][C:20]2=1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 68110ChromanoneHCID 3016725(4-(Benzyloxy)phenyl)hydrazine monohydrochloride

Product 1

HCID 59676133HCID 59676133, compound

Procedure

Following the procedure described in Example 4, using (4-benzyloxy-phenyl)-hydrazine hydrochloride salt and Chroman-4-one (2.93 g, 16.84 mmol) as the starting material, the title compound was prepared as a brown solid.

Sources & evidence

ORD record
ord-cd3ed3eeaf9d4aa5b0e364d76ca4523a
Source dataset
uspto-grants-2012_11
Patent number
US08318766B2

Reaction notes

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