HCID 59676083, compound → HCID 59676088, compound

HRID 1880450Notes

Reaction equation

HRID 1880450 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[N:9]([CH3:13])[CH2:8][C:7]1[C:14]3[C:19]([N:20]([CH3:21])[C:6]2=1)=[CH:18][CH:17]=[C:16]([O:22]C)[CH:15]=3.CN1C2C(=CC(O)=CC=2)C2N(C)C3C(C=2C1)=CC(O)=CC=3>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[N:9]([CH3:13])[CH2:8][C:7]1[C:14]3[C:19]([N:20]([CH3:21])[C:6]2=1)=[CH:18][CH:17]=[C:16]([OH:22])[CH:15]=3

Participants

3

Reactant 2

HCID 59676083HCID 59676083, compoundHCID 59676130HCID 59676130, compound

Product 1

HCID 59676088HCID 59676088, compound

Procedure

Following the procedure in Example 58, using 2,8-dimethoxy-5,11-dimethyl-5,11-dihydro-6H-indolo[3,2-c]quinoline (150 mg) as the starting material, 5,11-dimethyl-5,11-dihydro-6H-indolo[3,2-c]quinoline-2,8-diol as was obtained a brown solid and 2-methoxy-5,11-dimethyl-5,11-dihydro-6H-indolo[3,2-c]quinolin-8-ol was obtained as a white solid.

Workup

  1. customas was obtained a brown solid

Sources & evidence

ORD record
ord-5174768f1dce4020b6b36c4b75c7ae72
Source dataset
uspto-grants-2012_11
Patent number
US08318766B2

Reaction notes

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