HCID 59676097, compound → HCID 59676060, compound

HRID 1880470Notes

Reaction equation

HRID 1880470 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[NH:15][C:14]3[C:13]4[CH:16]=[CH:17][CH:18]=[CH:19][C:12]=4[S:11][CH2:10][CH2:9][C:8]=3[C:7]=2[CH:20]=1.Cl.Cl[CH2:23][C:24]1[CH:38]=[CH:37][C:27]([O:28][CH2:29][CH2:30][NH:31][CH:32]2C[CH2:35][CH2:34][CH2:33]2)=[CH:26][CH:25]=1>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[N:15]([CH2:23][C:24]3[CH:25]=[CH:26][C:27]([O:28][CH2:29][CH2:30][N:31]4[CH2:32][CH2:33][CH2:34][CH2:35]4)=[CH:37][CH:38]=3)[C:14]3[C:13]4[CH:16]=[CH:17][CH:18]=[CH:19][C:12]=4[S:11][CH2:10][CH2:9][C:8]=3[C:7]=2[CH:20]=1

Participants

3

Reactant 2

HCID 59676097HCID 59676097, compoundHCID 67238454HCID 67238454, compound

Product 1

HCID 59676060HCID 59676060, compound

Procedure

Following the same procedure in Example 102, using 9-methoxy-6,7-dihydro-12H-5-thia-12-aza-dibenzo[a,e]azulene (562 mg) and [2-(4-chloromethyl-phenoxy)-ethyl]-cyclopentyl-amine hydrochloride salt as the starting material, the title compound was prepared as a brown solid.

Sources & evidence

ORD record
ord-e04279b9dbaa4661a5ab7ac6bb12b1da
Source dataset
uspto-grants-2012_11
Patent number
US08318766B2

Reaction notes

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