HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57446951, compound → HCID 13675226, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57446951 | HCID 57446951 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13675226 | HCID 13675226 | — |
Reaction Steps
The above alcohol was dissolved in EtOH (150 mL) and 10% Pd/C (˜500 mg) was added. The mixture was stirred under a H2 atmosphere (ballon) overnight. The catalyst was filtered off through celite and the filtrate was concentrated to give the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318748B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-058772b808db47c5b7e81a6ac0a8d294 |
| Source note | uspto-grants-2012_11 |