HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → HCID 67094269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 13837927 | HCID 13837927 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 67094269 | HCID 67094269 | — |
Reaction Steps
A solution of 2-bromomethyl-4,5-dimethoxy-benzoic acid methyl ester (2.9 g), 4-chloroaniline (1.28 g) and triethylamine (1.4 ml) was refluxed in toluene for six hours. The reaction mixture was stirred in an ice bath, filtered and washed with 1 M hydrochloric acid and water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318785B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-45a12d2fb7b44a2eb5f54fc0d27135e8 |
| Source note | uspto-grants-2012_11 |