HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzothiazole, 5,6-dimethoxy-2-methyl- → 2-methyl-1,3-benzothiazole-5,6-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzothiazole, 5,6-dimethoxy-2-methyl- | HCID 112829 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | 2-methyl-1,3-benzothiazole-5,6-diol | HCID 736940 | — |
Reaction Steps
5,6-Dimethoxy-2-methyl-benzothiazole (3.9 g) was refluxed with 47% hydrobromic acid (40 ml) for four hours. The solid was filtered and dried under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318785B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-eeadfb548c31404dabcabe946cb10da2 |
| Source note | uspto-grants-2012_11 |