HCID 67094264, compound → HCID 67094202, compound

HRID 1881200Notes

Reaction equation

C([O:4][C:5]1[C:15]([O:16][C:17](=[O:19])[CH3:18])=[CH:14][C:8]2[C:9](=[O:13])[N:10]([CH3:12])[S:11][C:7]=2[CH:6]=1)(=O)C>N1CCOCC1.CN(C)C=O>[OH:4][C:5]1[C:15]([O:16][C:17](=[O:19])[CH3:18])=[CH:14][C:8]2[C:9](=[O:13])[N:10]([CH3:12])[S:11][C:7]=2[CH:6]=1

Participants

Conditions

Temperature: 0 °C

Procedure

To a solution of acetic acid 6-acetoxy-2-methyl-3-oxo-2,3-dihydro-benzo[d]isothiazol-5-yl ester (0.21 g) in dimethylformamide morpholine (0.070 g) was added at 0° C. The mixture was stirred at 0° C. for one hour and then poured to ice water. The precipitated product was filtered.

Workup

filtrationThe precipitated product was filtered

Sources & evidence

ORD record: ord-900211e2789b4e8888dd9b3864669367
Source dataset: uspto-grants-2012_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08318785B2

Reaction notes

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