Water → HCID 86633447, compound

Participants

Reaction Steps

2-Bromo-3,4-dihydroxy-5-nitrobenzaldehyde (5.2 g), ethylbromide (4.5 ml) and N,N-diisopropylethylamine (10.5 ml) in N,N-dimethylformamide (50 ml) were stirred at 70° C. for 2 days. The mixture was poured into water and extracted with ether. The organic phase was washed with NaOH-solution, dried with Na2SO4 and evaporated to dryness.

Provenance & Evidence