Hydrochloric Acid → HCID 67094366, compound

Participants

Reaction Steps

To a solution of 2-bromo-3,4-diethoxy-5-nitrobenzaldehyde (1.5 g) in N,N-dimethylformamide (5 ml) were added methyl thioglycolate (1.5 g) and triethylamine (2.2 ml) at 0° C. Stirring was continued at room temperature overnight. 1 M HCl was added and the product was extracted with ether. The organic phase was dried with Na2SO4 and evaporated. The crude product was triturated with methanol.

Provenance & Evidence