HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 178473354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-Oxo-2,3-dihydro-1H-indole-5-carbonitrile | HCID 2773346 | — |
| Reactant | 2-Chloro-5-(((3aS,6aS)-5-(ethoxycarbonyl)hexahydropyrrolo[3,4-b]pyrrol-1(2H)-yl)methyl)pyridine 1-oxide | HCID 86649563 | — |
| Product | HCID 178473354 | HCID 178473354 | — |
Reaction Steps
The titled compound was prepared in analogy to example 4.1 using sodium hydride on mineral oil (101 mg, 2.53 mmol), 2-oxoindoline-5-carbonitrile (300 mg, 1.897 mmol), and 2-chloro-5-(((3aS,6aS)-5-(ethoxycarbonyl)hexahydropyrrolo[3,4-b]pyrrol-1(2H)-yl)methyl)pyridine 1-oxide (412, 1.265 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318793B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-ebc752c3e48e49f8a5f36e428380f163 |
| Source note | uspto-grants-2012_11 |