HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Methoxycarbonyl-3-nitrobenzhydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Methyl hydrogen 2-nitroterephthalate | HCID 98592 | — |
| Product | 4-Methoxycarbonyl-3-nitrobenzhydrazide | HCID 66986356 | — |
Reaction Steps
From 4-methoxycarbonyl-3-nitrobenzoic acid, thionyl chloride and hydrazine monohydrate, 758 mg of the desired product was obtained in the same manner as in Reference Synthetic Example 39 as a white solid (yield 79%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318796B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-50098fa320cb458f8764c0f11e5e4c63 |
| Source note | uspto-grants-2012_11 |